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![]() Atacama's Qualified Person pursuant to NI-43-101 is Mr. Ron F. Hochstein, P. Eng., MBA. Mr. Hochstein is a Director of the Company. Aguas Blancas Assay methods are extracted from the Aguas Blancas NI 43-101 Technical Report dated December, 2007. Each bagged sample (approximately 10kg) from the reverse circulation, equivalent to 0.5m of drilling, is sent to the sample preparation facility at Aguas Blancas. Here the following steps are completed:
Since July 2005, samples have been prepared and subsequently analysed on site in the new laboratory facilities. Sulphates and nitrates have similarly been analysed in the on-site laboratory, using volumetric techniques, since November 2005. Since April 2006, sulphates have been analysed using ICP equipment (inductively coupled plasma optimal emission spectroscopy), and nitrates using Molecular Absorption (MA) Equipment. ISO9001 certification has also been obtained, which includes the new on-site laboratory facilities. For iodine measurement, the method used is very similar to that used in external laboratories. The main methods of assay measurement are summarised below: Iodine 10g sample, leached with hot water and then filtered. Acid and chlorine added to the filtered solution. Heat applied on heating plate, then cooled. Starch added and then titration with sodium thiosulphate. Sulphates 5g sample, leached with hot water, filtered. 2ml fraction taken, 1ml of acid added 1ml of standard Yttrium, before taking ICP reading. Nitrates 5g sample, leached with hot water and filtered to 250ml. Solution out into quartz cell and then reading taken with MA instrument. When the on-site laboratory was being commissioned, a set of 20 check samples (CS) were made with respect to iodine measurements, and sent to 3 different external labs. These results are discussed in more detail in Section 14. For the iodine measurements, the sodium thiosulphate is checked every day, with a standard of potassium iodate (KIO3) -- standard sample (SS). For the nitrate and sulphate measurements using the ICP and Molecular Absorption Equipment, the following QA/QC steps are taken:
It is the author's (Adam Wheeler, C.Eng., Eur.Ing. Consulting Mining Engineer) opinion that the sample preparation and analytical procedures used by Atacama are adequate for resource and reserve estimation purposes. |
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